H-Lys-OMe*HCl

Base Information

• Chemical Name: H-Lys-OMe*HCl
• CAS No.: 73995-27-4
• Molecular Formula: C₁₅H₂₁ClN₂O₄*ClH
• Molecular Weight: 365.257

Synonyms:H-Lys-OMe*HCl

Chemical Property of H-Lys-OMe*HCl

Chemical Property:

Purity/Quality:

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Technology Process of H-Lys-OMe*HCl

There total 2 articles about H-Lys-OMe*HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + Boc-(S)-Lys(2-Cl-Z)-OH (54613-99-9) → H-Lys-OMe*HCl (73995-27-4)

Guidance literature:

With thionyl chloride; at 0 - 20 ℃;

DOI:10.1002/ejoc.201000123

Reference yield: 70.6%

methanol (67-56-1) + Nε-(2-Chlorophenylmethoxycarbonyl)-(S)-lysine (42390-97-6,201014-19-9) → H-Lys-OMe*HCl (73995-27-4)

Guidance literature:

With thionyl chloride; for 72h; Ambient temperature;

DOI:10.1246/bcsj.53.192

Reference yield: 83.6%

Boc-Gln-ONp (15387-45-8) + H-Lys-OMe*HCl (73995-27-4) → Boc-Gln-Lys-OMe (73995-28-5)

Guidance literature:

With TEA; In N,N-dimethyl-formamide; for 24h; Ambient temperature;

DOI:10.1246/bcsj.53.192

upstream raw materials:

methanol

N^ε-(2-Chlorophenylmethoxycarbonyl)-(S)-lysine

Boc-(S)-Lys(2-Cl-Z)-OH

Downstream raw materials:

Boc-Gln-Lys-OMe

(S)-2-((S)-2-Amino-4-carbamoyl-butyrylamino)-6-(2-chloro-benzyloxycarbonylamino)-hexanoic acid methyl ester

(S)-2-((S)-4-Carbamoyl-2-{[(S)-1-((S)-pyrrolidine-2-carbonyl)-pyrrolidine-2-carbonyl]-amino}-butyrylamino)-6-(2-chloro-benzyloxycarbonylamino)-hexanoic acid methyl ester

Boc-Pro-Pro-Gln-Lys-OMe

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