(E)-2-methoxy-N-3-phenylacryloylbenzamide

Base Information

Chemical Name:(E)-2-methoxy-N-3-phenylacryloylbenzamide
CAS No.:906126-80-5
Molecular Formula:C₁₇H₁₅NO₃
Molecular Weight:281.311
Hs Code.:

Synonyms:(E)-2-methoxy-N-3-phenylacryloylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-methoxy-N-3-phenylacryloylbenzamide

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Technology Process of (E)-2-methoxy-N-3-phenylacryloylbenzamide

There total 1 articles about (E)-2-methoxy-N-3-phenylacryloylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 2439-77-2
2-methoxybenzamide

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 906126-80-5
(E)-2-methoxy-N-3-phenylacryloylbenzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; copper(l) chloride; In dichloromethane; for 1h;
DOI:10.1021/ja061364f

Reference yield: 53.0%

: 906126-80-5
(E)-2-methoxy-N-3-phenylacryloylbenzamide

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: C₂₅H₂₄N₂O₃

Guidance literature:: With 1-(3,5-bis-trifluoromethyl-phenyl)-3-{2'-[3-(3,5-bis-trifluoromethyl-phenyl)-thioureido]-[1,1']binaphthalenyl-2-yl}-thiourea; 2,2’-azobis(4-methoxy-2,4-dimethyl)valeronitrile; C₃₆H₂₂F₁₀IrN₄O₂⁽¹⁺⁾*BF₄^(1-); at 20 ℃; for 25h; diastereoselective reaction; Inert atmosphere; Irradiation;
DOI:10.1002/chem.202004186

Reference yield:

: 906126-80-5
(E)-2-methoxy-N-3-phenylacryloylbenzamide

: 67-56-1
methanol

: 105-34-0
methyl 2-cyanoacetate

: (3R)-4-cyano-3-phenylbutanoic acid methyl ester

: (3S)-4-cyano-3-phenylbutanoic acid methyl ester

Guidance literature:: (E)-2-methoxy-N-3-phenylacryloylbenzamide; methyl 2-cyanoacetate; chiral thiourea; In toluene; at 80 ℃; for 52h;

methanol; erbium(III) triflate; at 0 ℃; for 4h;

With sodium chloride; In water; N,N-dimethyl-formamide; at 130 ℃; for 24h; Title compound not separated from byproducts;
DOI:10.1021/ja061364f