(5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III)

Base Information

Chemical Name:(5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III)
CAS No.:874299-58-8
Molecular Formula:C₅₅H₄₁N₄ORh
Molecular Weight:876.862
Hs Code.:

Synonyms:(5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III)

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Chemical Property of (5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III)

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Technology Process of (5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III)

There total 20 articles about (5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1247874-33-4
Rh(ttp)CH₂COPh

: 874299-58-8
(5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III)

Guidance literature:: at 200 ℃; for 168h; Inert atmosphere; Darkness;
DOI:10.1021/om1007852

Reference yield: 99.0%

: 103562-44-3
(5,10,15,20-tetrakis-4-tolylporphyrinato)rhodium(III) hydride

: 98-86-2
acetophenone

: 874299-58-8
[Rh(5,10,15,20-tetratolylporphyrinato)(COPh)]

Guidance literature:: In neat (no solvent); (N2); heating of freshly prepared RhH(5,10,15,20-tetratolylporphyrinato)and acetophenone at 200°C under N2 for 7 ds in the dark; monitoring by TLC for 30 min, drying under vac., silica gel column chromy. with hexane/CH2Cl2 as eluent;
DOI:10.1021/om200788p