N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide

Base Information

Chemical Name:N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide
CAS No.:460049-38-1
Molecular Formula:C₃₀H₃₄N₄O₅
Molecular Weight:530.624
Hs Code.:

Synonyms:N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide

Suppliers and Price of N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide

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Technology Process of N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide

There total 2 articles about N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.7%

: 100-52-7
benzaldehyde

: 100-46-9
benzylamine

: 543-24-8
N-acetylglycine

: 460048-60-6
formic acid 1-benzylcarbamoyl-2-isocyano-propyl ester

: 460049-38-1
N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide

Guidance literature:: In methanol; dichloromethane; at 20 ℃; for 48h;
DOI:10.1055/s-2002-31948

Reference yield:

: 460049-36-9
N-benzyl-2-formyloxy-3-formamidobutyric amide

: 460049-38-1
N-benzyl-2-hydroxy-3-[acetylglycyl-(N-benzyl-2-phenyl)glycyl]aminobutyric amide

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃; Et₃N / CH₂Cl₂ / 0.5 h

2: 33.7 percent / methanol; CH₂Cl₂ / 48 h / 20 °C

With triethylamine; trichlorophosphate; In methanol; dichloromethane; 2: Ugi reaction;
DOI:10.1055/s-2002-31948