C₂₆H₄₀N₂O₃SSi

Base Information

• Chemical Name: C₂₆H₄₀N₂O₃SSi
• CAS No.: 157734-21-9
• Molecular Formula: C₂₆H₄₀N₂O₃SSi
• Molecular Weight: 488.767
• Mol file: 157734-21-9.mol

Synonyms:C₂₆H₄₀N₂O₃SSi

Chemical Property of C₂₆H₄₀N₂O₃SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₄₀N₂O₃SSi

There total 3 articles about C₂₆H₄₀N₂O₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

tert-butyldimethylsilyl chloride (18162-48-6) + N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide (157734-20-8) → C26H40N2O3SSi (157734-21-9)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 45 ℃; for 48h;

DOI:10.1246/bcsj.67.1855

Reference yield:

styrene oxide (96-09-3) → C26H40N2O3SSi (157734-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) BuLi / 1.) ether, hexane, RT, 30 min, 2.) ether, hexane, 12 h

2: 91 percent / imidazole / dimethylformamide / 48 h / 45 °C

With 1H-imidazole; n-butyllithium; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.67.1855

Reference yield:

N-(p-tolyl)methanesulfonimidomorpholide (76867-83-9) → C26H40N2O3SSi (157734-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) BuLi / 1.) ether, hexane, RT, 30 min, 2.) ether, hexane, 12 h

2: 91 percent / imidazole / dimethylformamide / 48 h / 45 °C

With 1H-imidazole; n-butyllithium; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.67.1855

upstream raw materials:

tert-butyldimethylsilyl chloride

N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

styrene oxide

N-(p-tolyl)methanesulfonimidomorpholide