C₁₅H₁₀Cl₂O

Base Information

• Chemical Name: C₁₅H₁₀Cl₂O
• CAS No.: 1092654-02-8
• Molecular Formula: C₁₅H₁₀Cl₂O
• Molecular Weight: 277.15
• Mol file: 1092654-02-8.mol

Synonyms:C₁₅H₁₀Cl₂O

Chemical Property of C₁₅H₁₀Cl₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₀Cl₂O

There total 2 articles about C₁₅H₁₀Cl₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

3,5-dichlorobenzaldehyde (10203-08-4) + (Benzoylmethylene)triphenylphosphorane (20913-05-7,859-65-4) → C15H10Cl2O (1092654-02-8)

Guidance literature:

at 20 - 27 ℃; for 24.0833h; Neat (no solvent); Air atmosphere;

DOI:10.1246/bcsj.80.1617

Reference yield: 75.0%

3',5'-dichloroacetophenone (14401-72-0) + benzaldehyde (100-52-7) → C15H10Cl2O (1092654-02-8)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; at 90 ℃; for 2h; Inert atmosphere;

Reference yield: 76.0%

pyridine (110-86-1) + C15H10Cl2O (1092654-02-8) + benzyl bromide (100-39-0) → (2-(3,5-dichlorophenyl)-3-phenylindolizin-1-yl)(phenyl)methanone

Guidance literature:

With oxygen; copper diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 8h;

DOI:10.1016/j.tet.2020.131347

upstream raw materials:

3,5-dichlorobenzaldehyde

(Benzoylmethylene)triphenylphosphorane

3',5'-dichloroacetophenone

benzaldehyde

Refernces

• 1、 -. "Synthesis method of chalcone derivative". Paragraph 0048-0050; 0081; 0082; 0088. . Retrieved 2020/07/03.