C₄₀H₅₂N₂O₆

Base Information

Chemical Name:C₄₀H₅₂N₂O₆
CAS No.:1351815-87-6
Molecular Formula:C₄₀H₅₂N₂O₆
Molecular Weight:656.863
Hs Code.:

C<sub>40</sub>H<sub>52</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₄₀H₅₂N₂O₆

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Chemical Property of C₄₀H₅₂N₂O₆

Chemical Property:

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Technology Process of C₄₀H₅₂N₂O₆

There total 9 articles about C₄₀H₅₂N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1351815-54-7
1-{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}piperidin-4-one

: 48067-24-9
O-tert-butyl L-serine tert-butyl ester

: 1351815-87-6
C₄₀H₅₂N₂O₆

Guidance literature:: 1-{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}piperidin-4-one; O-tert-butyl L-serine tert-butyl ester; With sodium tris(acetoxy)borohydride; In 1,1-dichloroethane; at 20 ℃; for 2h;

With sodium hydrogencarbonate; In 1,1-dichloroethane; water;

Reference yield:

: 912545-08-5
2,4-bis-benzyloxy-5-isopropenyl-benzoic acid methyl ester

: 1351815-87-6
C₄₀H₅₂N₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; methanol / 20 h / 75 °C

1.2: 0.5 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 23 h / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 20 °C

4.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 2 h / 20 °C

With methanol; sodium tris(acetoxy)borohydride; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In 1,1-dichloroethane; dichloromethane;

Reference yield:

: 2150-47-2
methyl 2,4-dihydroxybenzoate

: 1351815-87-6
C₄₀H₅₂N₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap / 1 h / 55 °C

2.1: trifluorormethanesulfonic acid / toluene / 2.5 h / 20 °C / Cooling with ice

2.2: 18 h / 20 °C

3.1: potassium carbonate / acetonitrile / 42 h / 75 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.5 h

4.2: 0.5 h

5.1: potassium hydroxide; methanol / 20 h / 75 °C

5.2: 0.5 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 23 h / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 20 °C

8.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 2 h / 20 °C

With methanol; trifluorormethanesulfonic acid; potassium tert-butylate; sodium tris(acetoxy)borohydride; potassium carbonate; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide; dmap; In tetrahydrofuran; 1,1-dichloroethane; dichloromethane; toluene; acetonitrile;