C₃₈H₅₆N₄O₈Si

Base Information

Chemical Name:C₃₈H₅₆N₄O₈Si
CAS No.:1353660-72-6
Molecular Formula:C₃₈H₅₆N₄O₈Si
Molecular Weight:724.97
Hs Code.:

C<sub>38</sub>H<sub>56</sub>N<sub>4</sub>O<sub>8</sub>Si

Synonyms:C₃₈H₅₆N₄O₈Si

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Chemical Property of C₃₈H₅₆N₄O₈Si

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Technology Process of C₃₈H₅₆N₄O₈Si

There total 11 articles about C₃₈H₅₆N₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1353660-68-0
C₃₉H₅₈N₄O₈Si

: C₃₂H₄₂N₄O₈

: 1353660-72-6
C₃₈H₅₆N₄O₈Si

Guidance literature:: C₃₉H₅₈N₄O₈Si; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;

With sodium hydrogen sulfate; In tetrahydrofuran; methanol; water; ethyl acetate; pH=Ca. 2;
DOI:10.1002/chem.201101978

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1353660-72-6
C₃₈H₅₆N₄O₈Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1H-imidazole / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with water bath

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -90 - -80 °C / Inert atmosphere

2.2: 0.5 h / -100 - -10 °C / Inert atmosphere

3.1: dichloromethane / 20 °C / Inert atmosphere

4.1: hydroquinidine 1 4-phthalazinediyl diether; potassium dioxotetrahydroxoosmate(VI); methanesulfonamide; water; potassium carbonate; potassium hexacyanoferrate(III) / tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

5.1: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / -25 - 20 °C / Inert atmosphere

6.1: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

8.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

9.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

9.2: pH Ca_. 2

With 1H-imidazole; hydroquinidine 1 4-phthalazinediyl diether; n-butyllithium; hydrogen azide; potassium dioxotetrahydroxoosmate(VI); methanesulfonamide; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium hydroxide; potassium hexacyanoferrate(III); diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 2.2: Wittig reaction / 3.1: Wittig reaction / 4.1: Sharpless dihydroxylation / 5.1: Mitsunobu reaction;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-41-9
(2S,3S)-methyl 3-azido-3-(4-(2-(tert-butyldimethylsilyloxy)ethyl)phenyl)-2-hydroxypropanoate

: C₃₂H₄₂N₄O₈

: 1353660-72-6
C₃₈H₅₆N₄O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

3.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

4.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

4.2: pH Ca_. 2

With palladium 10% on activated carbon; water; hydrogen; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101978