(4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:(4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)
CAS No.:945489-92-9
Molecular Formula:C₂₉H₃₆N₂O₉S₂
Molecular Weight:620.745
Hs Code.:

Synonyms:(4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)

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Chemical Property of (4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)

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Technology Process of (4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)

There total 5 articles about (4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 945489-93-0
tert-butyl (3-[(2,6-bis(hydroxymethyl)pyridin-4-yl)oxy]propyl)carbamate

: 98-59-9
p-toluenesulfonyl chloride

: 945489-92-9
(4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 16h;

Reference yield:

: 58885-58-8
N-tert-butoxycarbonyl-3-aminopropanol

: 945489-92-9
(4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12 h / 70 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 2 h / Reflux

3: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; ethanol; water; 1: |Mitsunobu Displacement;
DOI:10.1039/c2ob26452h

Reference yield:

: 68631-52-7
4-hydroxypyridine-2,6-dicarboxylic acid diethylester

: 945489-92-9
(4-(3-[(tert-butoxycarbonyl)amino]propoxy)pyridine-2,6-diyl)-bis(methylene)bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12 h / 70 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 2 h / Reflux

3: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; ethanol; water; 1: |Mitsunobu Displacement;
DOI:10.1039/c2ob26452h