4-chloro-3-nitrobenzenecarbothioamide

Base Information

Chemical Name:4-chloro-3-nitrobenzenecarbothioamide
CAS No.:871933-36-7
Molecular Formula:C₇H₅ClN₂O₂S
Molecular Weight:216.648
Hs Code.:

Synonyms:4-chloro-3-nitrobenzenecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-3-nitrobenzenecarbothioamide

Chemical Property:

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Technology Process of 4-chloro-3-nitrobenzenecarbothioamide

There total 3 articles about 4-chloro-3-nitrobenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 16588-06-0
4-chloro-3-nitrobenzamide

: 871933-36-7
4-chloro-3-nitrobenzenecarbothioamide

Guidance literature:: With Lawessons reagent; In 1,4-dioxane; at 110 ℃; for 2h;
DOI:10.1021/jm201546m

Reference yield: 90.0%

: 939-80-0
4-chloro-3-nitrobenzonitrile

: 871933-36-7
4-chloro-3-nitrobenzenecarbothioamide

Guidance literature:: 4-chloro-3-nitrobenzonitrile; With calcium hydride; tiolacetic acid; at 80 ℃; for 1h;

With water; In ethyl acetate; at 20 ℃;
DOI:10.1055/s-0029-1217711

Reference yield:

: 96-99-1
4-chloro-3-nitrobenzoate

: 871933-36-7
4-chloro-3-nitrobenzenecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / thionyl chloride / 1 h / Heating / reflux

1.2: 1 h

2.1: Lawessons reagent / tetrahydrofuran / 1 h / Heating / reflux

With Lawessons reagent; N,N-dimethyl-formamide; In tetrahydrofuran; thionyl chloride;