1,2,4,5-Tetraoxaspiro[5.5]undecane,3-methyl-3-(2-methylpropyl)-(9CI)

Base Information

Chemical Name:1,2,4,5-Tetraoxaspiro[5.5]undecane,3-methyl-3-(2-methylpropyl)-(9CI)
CAS No.:804548-92-3
Molecular Formula:C₁₂H₂₂O₄
Molecular Weight:230.304
Hs Code.:
Mol file:804548-92-3.mol

Synonyms:1,2,4,5-Tetraoxaspiro[5.5]undecane,3-methyl-3-(2-methylpropyl)-(9CI)

Suppliers and Price of 1,2,4,5-Tetraoxaspiro[5.5]undecane,3-methyl-3-(2-methylpropyl)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,2,4,5-Tetraoxaspiro[5.5]undecane,3-methyl-3-(2-methylpropyl)-(9CI)

Chemical Property:

PSA：36.92000
LogP:3.31910

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2,4,5-Tetraoxaspiro[5.5]undecane,3-methyl-3-(2-methylpropyl)-(9CI)

There total 3 articles about 1,2,4,5-Tetraoxaspiro[5.5]undecane,3-methyl-3-(2-methylpropyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1112-78-3
2,2-dimethoxy-4-methylpentane

: 2699-11-8
1,1-dihydroperoxycyclohexane

: 804548-92-3
3-isobutyl-3-methyl-1,2,4,5-tetraoxa-spiro[5.5]undecane

: 183-84-6
Cyclohexanone diperoxide

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 - 25 ℃; for 0.166667h; Further Variations:; Solvents; Temperatures; time; Product distribution;
DOI:10.1055/s-2004-831171

Reference yield: 13.26%

: 2699-11-8
1,1-dihydroperoxycyclohexane

: 108-10-1
4-methyl-2-pentanone

: 804548-92-3
3-isobutyl-3-methyl-1,2,4,5-tetraoxa-spiro[5.5]undecane

Guidance literature:: With sulfuric acid; In dichloromethane; acetonitrile; at 0 - 10 ℃; for 1.33333h;
DOI:10.1007/s11094-021-02500-2

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 804548-92-3
3-isobutyl-3-methyl-1,2,4,5-tetraoxa-spiro[5.5]undecane

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; hydrogenchloride / acetonitrile; dichloromethane; water / 2 h / 20 °C

2: sulfuric acid / acetonitrile; dichloromethane / 1.33 h / 0 - 10 °C

With hydrogenchloride; sulfuric acid; dihydrogen peroxide; In dichloromethane; water; acetonitrile;
DOI:10.1007/s11094-021-02500-2