3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol

Base Information

Chemical Name:3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol
CAS No.:160280-62-6
Molecular Formula:C₄₀H₅₄O₄
Molecular Weight:598.866
Hs Code.:

Synonyms:3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol

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Technology Process of 3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol

There total 10 articles about 3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

: 2,3-O-isopropylidene-5-O-triphenylmethyl-D-lyxofuranose

: 160280-62-6
3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol

Guidance literature:: With lithium hexamethyldisilazane; at -78 ℃;
DOI:10.1016/S0040-4039(03)01281-4

Reference yield:

: C₂₇H₂₈O₅

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

: 160280-62-6
3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol

Guidance literature:: C₂₇H₂₈O₅; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 1h; under 760.051 Torr; Inert atmosphere;

n-tridecyltriphenylphosphonium bromide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; for 10h; under 760.051 Torr;

Reference yield:

: 86657-56-9
n-tridecylidenetriphenylphosphorane

: 2,3-O-isopropylidene-5-O-triphenylmethyl-D-lyxofuranose

: 160280-62-6
3,4-O-isopropylidene-1-O-triphenylmethyl-D-arabino-octadec-5-en-1,2,3,4-tetraol

Guidance literature:: 2,3-O-isopropylidene-5-O-triphenylmethyl-D-lyxofuranose; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

n-tridecylidenetriphenylphosphorane; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 9h;