4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide

Base Information

Chemical Name:4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide
CAS No.:1204213-00-2
Molecular Formula:C₂₃H₁₅F₃N₄O₃S₂
Molecular Weight:516.524
Hs Code.:

Synonyms:4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide

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Chemical Property of 4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide

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Technology Process of 4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide

There total 2 articles about 4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2361-27-5
2-thienylhydrazide

: 897564-36-2
2-phenyl-6-trifluoromethoxyquinoline-4-carboxylic acid

: 333-20-0
potassium thioacyanate

: 1204213-00-2
4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide

Guidance literature:: 2-phenyl-6-trifluoromethoxyquinoline-4-carboxylic acid; With oxalyl dichloride; In dichloromethane; at 20 ℃; for 3h;

potassium thioacyanate; In acetonitrile; at 20 ℃; for 1h;

2-thienylhydrazide; In acetonitrile; at 20 ℃;

Reference yield:

: 169037-23-4
5-trifluoromethoxy-1H-indole-2,3-dione

: 1204213-00-2
4-(2-phenyl-6-trifluoromethoxy-4-quinolinecarbonyl)-1-(2-thiophenecarbonyl)thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 1 h / Cooling with ice; Reflux

2.1: oxalyl dichloride / dichloromethane / 3 h / 20 °C

2.2: 1 h / 20 °C

2.3: 20 °C

With oxalyl dichloride; potassium hydroxide; In ethanol; dichloromethane;