Technology Process of N-(4-chloro-3-sulfamoylphenyl)formamide
There total 4 articles about N-(4-chloro-3-sulfamoylphenyl)formamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / water / 1 h / 20 °C
2: chlorosulfonic acid / 4 h / 5 - 130 °C
3: ammonia / water / 10 - 20 °C
4: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 50 °C
5: formic acid / tetrahydrofuran / 10 h / 20 °C
With
chlorosulfonic acid; formic acid; palladium 10% on activated carbon; ammonia; hydrogen; sodium hydroxide;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/j.ejmech.2012.01.011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: chlorosulfonic acid / 4 h / 5 - 130 °C
2: ammonia / water / 10 - 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 50 °C
4: formic acid / tetrahydrofuran / 10 h / 20 °C
With
chlorosulfonic acid; formic acid; palladium 10% on activated carbon; ammonia; hydrogen;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/j.ejmech.2012.01.011
- Guidance literature:
-
Multi-step reaction with 6 steps
1: fuming sulphuric acid / 6 h / 0 - 115 °C
2: sodium hydroxide / water / 1 h / 20 °C
3: chlorosulfonic acid / 4 h / 5 - 130 °C
4: ammonia / water / 10 - 20 °C
5: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 50 °C
6: formic acid / tetrahydrofuran / 10 h / 20 °C
With
chlorosulfonic acid; formic acid; fuming sulphuric acid; palladium 10% on activated carbon; ammonia; hydrogen; sodium hydroxide;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/j.ejmech.2012.01.011
