2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide

Base Information

Chemical Name:2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide
CAS No.:1039456-28-4
Molecular Formula:C₂₂H₃₇NO₅Si
Molecular Weight:423.625
Hs Code.:

Synonyms:2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide

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Technology Process of 2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide

There total 1 articles about 2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1039456-14-8
ethyl 2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)acetate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1039456-28-4
2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide

Guidance literature:: With isopropylmagnesium chloride; In tetrahydrofuran; diethyl ether; at -20 ℃; for 0.5h;
DOI:10.1021/ol801055b

Reference yield: 90.0%

: 1039456-28-4
2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide

: 75-16-1
methylmagnesium bromide

: 1039456-12-6
1-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)propan-2-one

Guidance literature:: 2-((2S,4S,6S)-6-(2-(tert-butyldimethylsilyloxy)ethyl)-2-phenyl-1,3-dioxan-4-yl)-N-methoxy-N-methylacetamide; methylmagnesium bromide; In tetrahydrofuran; at -78 - 20 ℃;

With water; ammonium chloride; In tetrahydrofuran;
DOI:10.1021/ol801055b