1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

Base Information

Chemical Name:1-<amino>-4,8-bis-11-amino-4,8-diazaundecane
CAS No.:151915-13-8
Molecular Formula:C₄₇H₆₈N₄O₈S₄
Molecular Weight:945.343
Hs Code.:

1-<<N-(2-mesitylene)sulfonyl>amino>-4,8-bis<N-(2-mesitylene)sulfonyl>-11-<N-ethyl-N-(2-mesitylene)sulfonyl>amino-4,8-diazaundecane

Synonyms:1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

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Chemical Property of 1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

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Technology Process of 1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

There total 11 articles about 1-<amino>-4,8-bis-11-amino-4,8-diazaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 151915-12-7
1-amino-4,8-bis-11-amino-4,8-diazaundecane

: 151915-13-8
1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

Guidance literature:: With sodium hydroxide; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jm00072a020

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 151915-13-8
1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, RT, 8 h, 2.) DMF, 70 deg C, 48 h

With sodium hydroxide; sodium hydride; In dichloromethane;
DOI:10.1021/jm00047a004

Reference yield:

: 151915-07-0
N-ethyl-(2-mesitylene)sulfonamide

: 151915-13-8
1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaH / 1.) DMF, 0 deg C, 2.) DMF, THF, RT, 4 h

2: 96 percent / NaH / dimethylformamide / 0.5 h / 0 °C

3: 75.5 percent / H₂ / 10percent Pd/C / CHCl₃; methanol / 48 h / 2585.7 Torr / Ambient temperature

4: 61 percent / 10percent aq. NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

5: 100 percent / hydrazine / methanol / 18 h / 50 °C

6: 50 percent / 10percent aq. NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium hydroxide; hydrogen; sodium hydride; hydrazine; palladium on activated charcoal; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00072a020