3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

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Chemical Name:3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one
CAS No.:1356920-05-2
Molecular Formula:C₂₈H₂₅N₅O₆S
Molecular Weight:559.602
Hs Code.:

Synonyms:3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

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Chemical Property of 3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

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Technology Process of 3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

There total 1 articles about 3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1008742-67-3
3-{4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

: 555-16-8
4-nitrobenzaldehdye

: 1356920-05-2
3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: 3-{4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one; With titanium tetrachloride; In dichloromethane; at 0 - 25 ℃; for 0.333333h; Inert atmosphere;

With N,N,N,N,-tetramethylethylenediamine; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

4-nitrobenzaldehdye; In dichloromethane; at 0 - 25 ℃; for 2h; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 1356920-05-2
3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

: 1356920-06-3
3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; at 25 ℃; for 1h; under 2585.81 Torr; Parr apparatus;

Reference yield:

: 1356920-05-2
3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

: 1356920-08-5
N-{4-[(1S,2S)-2-{[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]carbonyl}-1-hydroxy-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butyl]phenyl}-4-ethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 1 h / 25 °C / 2585.81 Torr / Parr apparatus

2: triethylamine / dichloromethane / 0.5 h / 0 °C

With hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;