3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

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Chemical Name:3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one
CAS No.:1356920-06-3
Molecular Formula:C₂₈H₂₇N₅O₄S
Molecular Weight:529.619
Hs Code.:

Synonyms:3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

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Chemical Property of 3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

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Technology Process of 3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

There total 3 articles about 3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356920-05-2
3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-hydroxy(4-nitrophenyl)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

: 1356920-06-3
3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; at 25 ℃; for 1h; under 2585.81 Torr; Parr apparatus;

Reference yield:

: 1008742-67-3
3-{4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

: 1356920-06-3
3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium tetrachloride / dichloromethane / 0.33 h / 0 - 25 °C / Inert atmosphere

1.2: 0.33 h / 0 °C / Inert atmosphere

1.3: 2 h / 0 - 25 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 1 h / 25 °C / 2585.81 Torr / Parr apparatus

With hydrogen; titanium tetrachloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1356920-06-3
3-[(3S,4S)-4-(4-aminophenyl)-3-{[(4S)-4-benzyl-2-oxo1,3-thiazolidin-3-yl]carbonyl}-4-hydroxybutyl]-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium tetrachloride / dichloromethane / 0.33 h / 0 - 25 °C / Inert atmosphere

1.2: 0.33 h / 0 °C / Inert atmosphere

1.3: 2 h / 0 - 25 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 1 h / 25 °C / 2585.81 Torr / Parr apparatus

With hydrogen; titanium tetrachloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;