1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea

Base Information

Chemical Name:1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea
CAS No.:1145355-37-8
Molecular Formula:C₁₅H₁₃ClFN₃O₂S
Molecular Weight:353.805
Hs Code.:

Synonyms:1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea

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Chemical Property of 1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea

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Technology Process of 1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea

There total 1 articles about 1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2339-58-4
3-fluoro-5-methoxyphenylamine

: 26413-58-1
2-chloro-6-methyl-4-pyridinecarbonyl chloride

: ammonium thiocyanate

: 1145355-37-8
1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea

Guidance literature:: 2-chloro-6-methyl-4-pyridinecarbonyl chloride; ammonium thiocyanate; In acetone; at 20 ℃; for 1h;

3-fluoro-5-methoxyphenylamine; In acetone; at 20 ℃; for 4h;

Reference yield: 84.3%

: 1145355-37-8
1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea

: 74-88-4
methyl iodide

: 1145355-38-9
1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-2-methyl-isothiourea

Guidance literature:: 1-(2-chloro-6-methyl-pyridine-4-carbonyl)-3-(3-fluoro-5-methoxy-phenyl)-thiourea; With sodium hydride; In tetrahydrofuran; paraffin oil (nujol); at 0 ℃; for 0.25h;

methyl iodide; In tetrahydrofuran; paraffin oil (nujol); at 20 ℃;