pent-4-ene-1-thiol

Base Information

• Chemical Name: pent-4-ene-1-thiol
• CAS No.: 17651-37-5
• Molecular Formula: C₅H₁₀S
• Molecular Weight: 102.2
• Mol file: 17651-37-5.mol

Synonyms:pent-4-ene-1-thiol

Chemical Property of pent-4-ene-1-thiol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pent-4-ene-1-thiol

There total 1 articles about pent-4-ene-1-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-pentenyl-1-amine (22537-07-1) → sulfure de pentamethylene (1613-51-0) + 2-methylthiolane (1795-09-1) + diamyl sulfide (872-10-6) + n-pentanethiol (110-66-7) + pent-4-ene-1-thiol (17651-37-5)

Guidance literature:

With hydrogen sulfide; hydrogen; sulfidized Ni-W; at 300 ℃; for 5h; Product distribution;

Reference yield: 44.0%

pent-4-ene-1-thiol (17651-37-5) + Diphenylphosphinic chloride (1499-21-4) → C17H19OPS

Guidance literature:

pent-4-ene-1-thiol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere;

Diphenylphosphinic chloride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2008.08.108

Reference yield: 9.0%

pent-4-ene-1-thiol (17651-37-5) → 2-methylthiolane (1795-09-1)

Guidance literature:

With Togni's reagent II; trifluoroacetic acid; In chloroform; at 20 ℃; for 24h;

DOI:10.1039/c6sc02790c

upstream raw materials:

4-pentenyl-1-amine

Downstream raw materials:

1-Methyl-4-[1-(pent-4-ene-1-sulfonylmethyl)-vinylsulfanyl]-benzene

1-Methyl-4-[3-(pent-4-ene-1-sulfonyl)-prop-1-ene-2-sulfonyl]-benzene

2-methylthiolane