5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine

Base Information

Chemical Name:5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine
CAS No.:1372854-80-2
Molecular Formula:C₂₂H₂₉N₃O₉
Molecular Weight:479.487
Hs Code.:

Synonyms:5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine

Chemical Property:

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Technology Process of 5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine

There total 7 articles about 5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₆₅N₃O₁₁Si₂

: 1372854-80-2
5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine

Guidance literature:: With ammonium fluoride; In methanol; at 50 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201106516

Reference yield:

: 1372854-34-6
(R/S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propanol

: 1372854-80-2
5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / dichloromethane / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 1 h / Reflux

3: 0.75 h / 110 °C / Inert atmosphere

4: ammonium fluoride / methanol / 12 h / 50 °C / Inert atmosphere

With dmap; ammonium fluoride; potassium carbonate; In methanol; dichloromethane;
DOI:10.1002/anie.201106516

Reference yield:

: 1372854-35-7
(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethyl-1-propyl (1S)-camphanate

: 1372854-80-2
5-[(S)-1-(5-methoxy-2-nitrophenyl)-2,2-dimethylpropyloxy]methyl-2’-deoxyuridine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol / 1 h / Reflux

2: 0.75 h / 110 °C / Inert atmosphere

3: ammonium fluoride / methanol / 12 h / 50 °C / Inert atmosphere

With ammonium fluoride; potassium carbonate; In methanol;
DOI:10.1002/anie.201106516