N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

Base Information

Chemical Name:N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide
CAS No.:871503-67-2
Molecular Formula:C₉H₇BrF₂INO
Molecular Weight:389.966
Hs Code.:

Synonyms:N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

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Chemical Property of N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

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Technology Process of N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

There total 2 articles about N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 871503-59-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

: 871503-67-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

Guidance literature:: With sodium iodide; In acetone; at 20 ℃; for 10h;
DOI:10.1016/j.jfluchem.2005.02.016

Reference yield:

: 104-94-9
4-methoxy-aniline

: 871503-67-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / PPh₃; Et₃N; CCl₄ / 5 h / Heating

2: 98 percent / NaI / acetone / 10 h / 20 °C

With tetrachloromethane; triethylamine; triphenylphosphine; sodium iodide; In acetone;
DOI:10.1016/j.jfluchem.2005.02.016

Reference yield: 81.0%

: 871503-67-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

: 5720-07-0
4-methoxyphenylboronic acid

: [2-Bromo-2,2-difluoro-1-(4-methoxy-phenyl)-eth-(E)-ylidene]-(4-methoxy-phenyl)-amine

Guidance literature:: With potassium carbonate; silver(l) oxide; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 70 ℃; for 8h;
DOI:10.1016/j.jfluchem.2005.02.016