N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

Base Information

Chemical Name:N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride
CAS No.:871503-59-2
Molecular Formula:C₉H₇BrClF₂NO
Molecular Weight:298.514
Hs Code.:

Synonyms:N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

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Chemical Property of N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

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Technology Process of N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

There total 1 articles about N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 354-08-5
bromodifluoroacetic acid

: 104-94-9
4-methoxy-aniline

: 871503-59-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

Guidance literature:: With tetrachloromethane; triethylamine; triphenylphosphine; for 5h; Heating;
DOI:10.1016/j.jfluchem.2005.02.016

Reference yield: 98.0%

: 871503-59-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

: 871503-67-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl iodide

Guidance literature:: With sodium iodide; In acetone; at 20 ℃; for 10h;
DOI:10.1016/j.jfluchem.2005.02.016

Reference yield:

: 871503-59-2
N-(p-anisyl)-2-bromo-2,2-difluoroacetimidoyl chloride

: bromodifluoromethyl-phenylketon-4-methoxyphenylimine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaI / acetone / 10 h / 20 °C

2: 79 percent / K₂CO₃; Ag₂O / PdCl₂(PPh₃)2 / tetrahydrofuran / 8 h / 70 °C

With potassium carbonate; sodium iodide; silver(l) oxide; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; acetone; 2: Suzuki coupling reaction;
DOI:10.1016/j.jfluchem.2005.02.016