2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:1151549-61-9
Molecular Formula:C₂₀H₃₁B₂FO₄
Molecular Weight:376.084
Hs Code.:

Synonyms:2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Chemical Property of 2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of 2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 4 articles about 2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 405-99-2
para-fluorostyrene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1151549-61-9
2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With zirconocene dichloride; lithium methanolate; In toluene; at 100 ℃; for 8h; under 760.051 Torr; Inert atmosphere;

Reference yield: 65.0%

: 459-46-1
4-Fluorobenzyl bromide

: 78782-17-9
4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane

: 1151549-61-9
2,2'-(2-(4-fluorophenyl)ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: 4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique; Sealed tube;

4-Fluorobenzyl bromide; With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/cjoc.202100701