(S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate

Base Information

Chemical Name:(S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate
CAS No.:153923-41-2
Molecular Formula:C₁₆H₂₅NO₆S
Molecular Weight:359.444
Hs Code.:

Synonyms:(S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate

Suppliers and Price of (S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate

There total 3 articles about (S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 124-63-0
methanesulfonyl chloride

: 126395-29-7
[(S)-2-hydroxy-1-(4-methoxybenzyl)ethyl]carbamic acid tert-butyl ester

: 153923-41-2
(S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at -3 ℃; for 5h;
DOI:10.1016/0040-4039(95)00039-F

Reference yield:

: 53267-93-9
O-methyl-N-tert-butoxycarbonyl-L-tyrosine

: 153923-41-2
(S)-2-[ (tert-butoxycarbonyl)-amino]-3-(4-methoxyphenyl)-propylmethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / BH₃*THF / tetrahydrofuran / 1.) 0 deg C, 1 h; 2.) RT; 3.) 0 deg C, 1 h

2: 97 percent / triethylamine / CH₂Cl₂ / 5 h / -3 °C

With borane-THF; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4039(95)00039-F