2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt

Base Information

Chemical Name:2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt
CAS No.:74514-61-7
Molecular Formula:C₂HF₃O₂*C₁₁H₁₃ClN₂O₅S
Molecular Weight:434.778
Hs Code.:

Synonyms:2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt

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Chemical Property of 2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt

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Technology Process of 2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt

There total 6 articles about 2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 74514-68-4
2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

: 76-05-1
trifluoroacetic acid

: 74514-61-7
2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt

Guidance literature:: In various solvent(s); at 0 ℃;
DOI:10.1021/ja00532a042

Reference yield:

: 937-32-6
4-nitrobenzenesulfenyl chloride

: 74514-61-7
2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, room temperature, overnight, 2.) room temperature, 30 min

2: 84 percent / various solvent(s) / 0 °C

With 3-chloro-benzenecarboperoxoic acid; In various solvent(s);
DOI:10.1021/ja00532a042

Reference yield:

: 1069-48-3,7685-44-1
rac-allylglycine

: 74514-61-7
2-amino-4-(p-nitrophenylsulfinyl)-5-chloropentanoic acid trifluoroacetyl salt

Guidance literature:: Multi-step reaction with 4 steps

1: 85.4 percent / triethylamine / H₂O; dioxane / 3.8 h / Ambient temperature

2: 80 percent / acetonitrile / 1 h / Ambient temperature

3: 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, room temperature, overnight, 2.) room temperature, 30 min

4: 84 percent / various solvent(s) / 0 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; water; acetonitrile;
DOI:10.1021/ja00532a042