2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

Base Information

Chemical Name:2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester
CAS No.:74514-68-4
Molecular Formula:C₂₉H₃₁ClN₂O₇S
Molecular Weight:587.093
Hs Code.:

Synonyms:2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

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Chemical Property of 2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

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Technology Process of 2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

There total 5 articles about 2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1069-48-3,7685-44-1
rac-allylglycine

: 74514-68-4
2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85.4 percent / triethylamine / H₂O; dioxane / 3.8 h / Ambient temperature

2: 80 percent / acetonitrile / 1 h / Ambient temperature

3: 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, room temperature, overnight, 2.) room temperature, 30 min

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; water; acetonitrile;
DOI:10.1021/ja00532a042

Reference yield:

: 100-32-3
di(p-nitrophenyl) disulfide

: 74514-68-4
2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Cl₂ / CCl₄ / 3 h / 60 °C

2: 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, room temperature, overnight, 2.) room temperature, 30 min

With chlorine; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane;
DOI:10.1021/ja00532a042

Reference yield:

: 119479-32-2
2-((tert-butyloxycarbonyl)amino)-4-pentenoic acid

: 74514-68-4
2-tert-Butoxycarbonylamino-5-chloro-4-(4-nitro-benzenesulfinyl)-pentanoic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / acetonitrile / 1 h / Ambient temperature

2: 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, room temperature, overnight, 2.) room temperature, 30 min

With 3-chloro-benzenecarboperoxoic acid; In acetonitrile;
DOI:10.1021/ja00532a042