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3-(tert-butyldiphenylsiloxymethyl)-4,4-dimethoxycyclohexa-2,5-dienone

Base Information Edit
  • Chemical Name:3-(tert-butyldiphenylsiloxymethyl)-4,4-dimethoxycyclohexa-2,5-dienone
  • CAS No.:1191391-89-5
  • Molecular Formula:C25H30O4Si
  • Molecular Weight:422.596
  • Hs Code.:
  • Mol file:1191391-89-5.mol
3-(tert-butyldiphenylsiloxymethyl)-4,4-dimethoxycyclohexa-2,5-dienone

Synonyms:3-(tert-butyldiphenylsiloxymethyl)-4,4-dimethoxycyclohexa-2,5-dienone

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 3-(tert-butyldiphenylsiloxymethyl)-4,4-dimethoxycyclohexa-2,5-dienone Edit
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Technology Process of 3-(tert-butyldiphenylsiloxymethyl)-4,4-dimethoxycyclohexa-2,5-dienone

There total 2 articles about 3-(tert-butyldiphenylsiloxymethyl)-4,4-dimethoxycyclohexa-2,5-dienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
methanol; tert-butyl((2,5-dimethoxybenzyl)oxy)diphenylsilane; With potassium hydroxide; at 0 ℃; Electrochemical reaction;
With acetic acid; In acetone; regioselective reaction;
DOI:10.1016/j.bmcl.2009.07.120
Guidance literature:
With acetic acid; In acetone; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201200878
Guidance literature:
With pyridinium p-toluenesulfonate; In benzene; Reflux;
DOI:10.1016/j.bmcl.2009.07.120
upstream raw materials:

methanol

tert-butyl((2,5-dimethoxybenzyl)oxy)diphenylsilane

C27H36O5Si

Downstream raw materials:

C26H30O4Si

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