N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine

Base Information

• Chemical Name: N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine
• CAS No.: 1012785-44-2
• Molecular Formula: C₁₇H₂₈BNO₂
• Molecular Weight: 289.226
• Hs Code.: 2931900090
• Mol file: 1012785-44-2.mol

Synonyms:N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine

Chemical Property of N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine

Chemical Property:

• Boiling Point: 363.8±25.0 °C(Predicted)
• PKA: 9.65±0.25(Predicted)
• Density: 0.98±0.1 g/cm3(Predicted)
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-(N,N-Diethylaminomethyl)phenylboronicacid,pinacolester ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine

There total 5 articles about N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diethylamine (109-89-7) + 4-bromomethylphenylboronic acid pinacol ester (138500-85-3) → N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine (1012785-44-2)

Guidance literature:

With PS-NMM; In tetrahydrofuran; at 150 ℃; for 0.25h; Microwave irradiation; in air;

DOI:10.1021/co100011g

Reference yield: 60.0%

→ N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine (1012785-44-2)

Guidance literature:

Reference yield:

1-(4-bromophenyl)-N,N-diethylmethanamine (4885-19-2) + bis(pinacol)diborane (73183-34-3) → N-ethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)ethanamine (1012785-44-2)

Guidance literature:

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 100 ℃; for 2.5h; Inert atmosphere;

DOI:10.1016/j.ejmech.2016.06.030

upstream raw materials:

diethylamine

4-bromomethylphenylboronic acid pinacol ester

1-bromomethyl-4-bromobenzene

1-(4-bromophenyl)-N,N-diethylmethanamine

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