methyl 2-fluoro-3-nitro-5-octylbenzoate

Base Information

Chemical Name:methyl 2-fluoro-3-nitro-5-octylbenzoate
CAS No.:1315305-54-4
Molecular Formula:C₁₆H₂₂FNO₄
Molecular Weight:311.353
Hs Code.:

Synonyms:methyl 2-fluoro-3-nitro-5-octylbenzoate

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Chemical Property of methyl 2-fluoro-3-nitro-5-octylbenzoate

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Technology Process of methyl 2-fluoro-3-nitro-5-octylbenzoate

There total 3 articles about methyl 2-fluoro-3-nitro-5-octylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 28741-08-4
n-octylboronic acid

: 1154278-17-7
methyl 5-bromo-2-fluoro-3-nitrobenzoate

: 1315305-54-4
methyl 2-fluoro-3-nitro-5-octylbenzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; at 90 ℃; for 30h; Inert atmosphere;
DOI:10.1021/ol201361f

Reference yield:

: 946126-94-9
2-fluoro-3-nitrobenzoic acid methyl ester

: 1315305-54-4
methyl 2-fluoro-3-nitro-5-octylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid / 6 h / 45 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 30 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; potassium carbonate; trifluoroacetic acid; In water; toluene;
DOI:10.1021/ol201361f

Reference yield:

: 317-46-4
2-fluoro-3-nitro-benzoic acid

: 1315305-54-4
methyl 2-fluoro-3-nitro-5-octylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 2 h / 60 °C

2: N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid / 6 h / 45 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 30 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; potassium carbonate; trifluoroacetic acid; In water; toluene;
DOI:10.1021/ol201361f