phenyl 1-trimethylsilylcrotyl sulfide

Base Information

• Chemical Name: phenyl 1-trimethylsilylcrotyl sulfide
• CAS No.: 78905-12-1
• Molecular Formula: C₁₃H₂₀SSi
• Molecular Weight: 236.453

Synonyms:phenyl 1-trimethylsilylcrotyl sulfide

Chemical Property of phenyl 1-trimethylsilylcrotyl sulfide

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Technology Process of phenyl 1-trimethylsilylcrotyl sulfide

There total 1 articles about phenyl 1-trimethylsilylcrotyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

chloro-trimethyl-silane (75-77-4) + (E)-but-2-en-1-yl phenyl sulfide (36195-56-9) → phenyl 1-trimethylsilylcrotyl sulfide (78905-12-1)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 3.5h;

Reference yield: 75.0%

phenyl 1-trimethylsilylcrotyl sulfide (78905-12-1) + butyryl chloride (141-75-3) → 3-methyl-1-phenylthio-1-hepten-4-one (78905-19-8)

Guidance literature:

aluminium trichloride; In dichloromethane; at -78 ℃; for 8h;

Reference yield: 75.0%

phenyl 1-trimethylsilylcrotyl sulfide (78905-12-1) + butyryl chloride (141-75-3) → (E)-3-Methyl-1-phenylsulfanyl-hept-1-en-4-one

Guidance literature:

With aluminium trichloride; In dichloromethane; at -78 ℃; for 8h;

DOI:10.1039/c39810000377

upstream raw materials:

chloro-trimethyl-silane

(E)-but-2-en-1-yl phenyl sulfide

Downstream raw materials:

3-methyl-1-phenylthio-1-octen-4-one

3-methyl-1-phenylthio-1-hepten-4-one

3-methyl-1-phenylthio-1-decen-4-one

3-methyl-1-phenylthio-1-undecen-4-one

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