tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate

Base Information

Chemical Name:tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate
CAS No.:1187450-65-2
Molecular Formula:C₃₂H₃₈N₆O₆S
Molecular Weight:634.756
Hs Code.:

Synonyms:tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate

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Chemical Property of tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate

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Technology Process of tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate

There total 10 articles about tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1187450-77-6
tert-butyl (tert-butoxycarbonyl{6-[(pyridin-3-ylsulfonyl)aminomethyl]pyridin-2-yl}amino)acetate

: 143426-49-7
1-(4-hydroxymethylphenyl)-1H-pyrazole

: 1187450-65-2
tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate

Guidance literature:: With tributylphosphine; diamide; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield: 92.0%

: 1187450-65-2
tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate

Guidance literature:

Reference yield:

: 1187451-25-7
tert-butyl [tert-butoxycarbonyl(6-ethoxycarbonylpyridine-2-yl)amino]acetate

: 1187450-65-2
tert-butyl (tert-butoxycarbonyl(6-((4-(pyrazol-1-yl)benzyl)(pyridin-3-ylsulfonyl)aminomethyl)pyridin-2-yl)amino)acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: ethanol; calcium chloride; sodium tetrahydroborate / Tetraethylene glycol dimethyl ether / 35 °C / Cooling with ice

1.2: 1.17 h / 29 °C / Cooling with ice

2.1: Dess-Martin periodane / dichloromethane / 2.33 h / 20 °C / Cooling with ice; Inert atmosphere

3.1: hydroxylamine hydrochloride; pyridine / 1 h / 20 °C

4.1: hydrogen / palladium / ethanol; water / 1 h / 20 °C / 760.05 Torr

5.1: triethylamine / dichloromethane / 1 h / 20 °C

6.1: tributylphosphine; diamide / tetrahydrofuran / 16 h / 20 °C

With pyridine; sodium tetrahydroborate; ethanol; tributylphosphine; diamide; hydroxylamine hydrochloride; hydrogen; Dess-Martin periodane; triethylamine; calcium chloride; palladium; In tetrahydrofuran; ethanol; dichloromethane; Tetraethylene glycol dimethyl ether; water;