2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine

Base Information

Chemical Name:2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine
CAS No.:127356-09-6
Molecular Formula:C₁₅H₁₅N₃O₃S
Molecular Weight:317.368
Hs Code.:

Synonyms:2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine

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Chemical Property of 2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine

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Technology Process of 2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine

There total 5 articles about 2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 127356-31-4
7-Methoxy-2-(2-methoxy-4-methylsulfanyl-phenyl)-1H-imidazo[4,5-c]pyridine

: 127356-09-6
2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at -15 ℃; for 1.5h;
DOI:10.1021/jm00170a030

Reference yield:

: 52334-90-4
4-amino-3-methoxy pyridine

: 127356-09-6
2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 37 percent / conc. H₂SO₄, HNO₃ / 3 h / 0 - 60 °C

2: 85 percent / H₂ / 10percent Pd/C / methanol

3: 25 percent / POCl₃ / 1.) RT, 0.5 h, 2.) reflux, 6 h

4: 72 percent / m-chloroperbenzoic acid / CHCl₃ / 1.5 h / -15 °C

With sulfuric acid; hydrogen; nitric acid; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jm00170a030

Reference yield:

: 19355-04-5
3-methoxy-4-nitropyridine 1-oxide

: 127356-09-6
2-(4-Methanesulfinyl-2-methoxy-phenyl)-7-methoxy-1H-imidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / H₂ / Raney Ni / methanol / 2.5 h / 40 °C / 30400 Torr

2: 37 percent / conc. H₂SO₄, HNO₃ / 3 h / 0 - 60 °C

3: 85 percent / H₂ / 10percent Pd/C / methanol

4: 25 percent / POCl₃ / 1.) RT, 0.5 h, 2.) reflux, 6 h

5: 72 percent / m-chloroperbenzoic acid / CHCl₃ / 1.5 h / -15 °C

With sulfuric acid; hydrogen; nitric acid; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; palladium on activated charcoal; nickel; In methanol; chloroform;
DOI:10.1021/jm00170a030