[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2][B(C₆H₃(CF₃)2)4]

Base Information

• Chemical Name: [RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2][B(C₆H₃(CF₃)2)4]
• CAS No.: 193205-75-3
• Molecular Formula: C₂₀H₄₅Cl₂OP₂Ru*C₃₂H₁₂BF₂₄
• Molecular Weight: 1398.72

Synonyms:[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2][B(C₆H₃(CF₃)2)4]

Chemical Property of [RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2][B(C₆H₃(CF₃)2)4]

Chemical Property:

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Technology Process of [RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2][B(C₆H₃(CF₃)2)4]

There total 2 articles about [RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[RuH(CO)(CH₂Cl₂)(P(C₄H₉)2CH₃)2][B(C₆H₃(CF₃)2)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

RuH(OTf)(CO)(P(t)Bu2Me)2 (193205-72-0) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [RuH(CO)(CH2Cl2)(P(C4H9)2CH3)2](1+)*[B(C6H3(CF3)2)4](1-)=[RuH(CO)(CH2Cl2)(P(C4H9)2CH3)2][B(C6H3(CF3)2)4] (193205-75-3)

Guidance literature:

In dichloromethane; (room temp., 5 min);

DOI:10.1021/ja970240n

Reference yield:

dichloromethane (75-09-2) + RuH(OTf)(CO)(Pt-Bu2Me)2 (193205-72-0) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [RuH(η2-CH2Cl2)(CO)(Pt-Bu2Me)2][B(3,5-C6H3(CF3)2)4] (193205-75-3)

Guidance literature:

In dichloromethane; react. RuH(OTf)(CO)(Pt-Bu2Me)2 with NaB(3,5-C6H3(CF3)2)4 in CH2Cl2; soln. was layered with pentane and kept at -20°C for 1 week, ppt. was filtered, washed with pentane and dried; elem. anal.;

DOI:10.1021/om9910017

Reference yield:

[RuH(η2-CH2Cl2)(CO)(Pt-Bu2Me)2][B(3,5-C6H3(CF3)2)4] (193205-75-3) → [RuH(CO)(P(t)Bu2Me)2]B(3,5-bis(trifluoromethyl)phenyl)4 (278168-30-2,193205-80-0)

Guidance literature:

In neat (no solvent, solid phase); crystals were pumped in vacuo for 12 h;

DOI:10.1021/om9910017

upstream raw materials:

dichloromethane

RuH(OTf)(CO)(Pt-Bu₂Me)2

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

RuH(OTf)(CO)(P(t)Bu₂Me)2

Downstream raw materials:

[RuH(OH₂)(CO)(Pt-Bu₂Me)2][B(3,5-C₆H₃(CF₃)2)4]

[RuH(CO)(P(t)Bu₂Me)2]B(3,5-bis(trifluoromethyl)phenyl)4

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