1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate

Base Information

Chemical Name:1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate
CAS No.:1248395-41-6
Molecular Formula:C₃₆H₃₇CuN₃O₂
Molecular Weight:607.255
Hs Code.:

Synonyms:1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate

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Chemical Property of 1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate

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Technology Process of 1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate

There total 1 articles about 1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1,8-diphenylimino-3,6-di-tert-butylcarbazole

: 6046-93-1
copper(II) acetate monohydrate

: 1248395-41-6
1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate

Guidance literature:: With CH₃COONa; In methanol; chloroform; addn. of soln. of copper compd. and sodium acetate in methanol to CHCl3 soln. of carbazole deriv., refluxing for 45 min; extn. (CH2Cl2), washing with water, drying over MgSO4, evapn., recrstn. (CH2Cl2/pentane), UV and MS;
DOI:10.1021/ic101170k

Reference yield: 99.0%

: 1248395-41-6
1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate

: 7647-14-5
sodium chloride

: 1248395-43-8
1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)chloride

Guidance literature:: In dichloromethane; water; addn. of aq. satd. soln. of NaCl to CH2Cl2 soln. of copper compd., stirrin for 3 h; isolation of organic layer, evapn., UV and MS;
DOI:10.1021/ic101170k

Reference yield:

: 1248395-41-6
1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(II)acetate

: 1,8-diphenylimino-3,6-di-tert-butylcarbazolide copper(I)

Guidance literature:: With (C₄H₉)4NClO₄; In benzonitrile; byproducts: CH3COO(1-); Electrochem. Process; electorchemical reduction of copper compd. in 0.2 M tetrabutylammonium perchlorate benzonitrile soln. at -1.20 V vs SCE; UV monitoring;
DOI:10.1021/ic101170k