C₃₄H₅₇NO₇Si

Base Information Edit

Chemical Name:C₃₄H₅₇NO₇Si
CAS No.:1392284-91-1
Molecular Formula:C₃₄H₅₇NO₇Si
Molecular Weight:619.915
Hs Code.:
Mol file:1392284-91-1.mol

C<sub>34</sub>H<sub>57</sub>NO<sub>7</sub>Si

Synonyms:C₃₄H₅₇NO₇Si

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Chemical Property of C₃₄H₅₇NO₇Si Edit

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Technology Process of C₃₄H₅₇NO₇Si

There total 33 articles about C₃₄H₅₇NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1392284-90-0
C₃₃H₅₅NO₇Si

: 74-88-4
methyl iodide

: 1392284-91-1
C₃₄H₅₇NO₇Si

Guidance literature:: C₃₃H₅₅NO₇Si; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.166667h;

methyl iodide; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.666667h;
DOI:10.1055/s-0033-1338493

Reference yield:

: 1392284-87-5
(2S,5R,7S)-7-[(tert-butyldimethylsilyl)oxy]-5-hydroxy-1-[(4-methoxybenzyl)oxy]-8-{4-[(S)-1-methoxybut-3-en-1-yl]oxazol-2-yl}-2,6,6-trimethyloctan-3-one

: 1392284-91-1
C₃₄H₅₇NO₇Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; dicyclohexylboron chloride / diethyl ether; tetrahydrofuran / 1.5 h / -30 °C

1.2: 1.5 h / -78 °C

1.3: 2 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

2.2: 0.67 h / 0 °C

With dicyclohexylboron chloride; sodium hydride; triethylamine; In tetrahydrofuran; diethyl ether; mineral oil;
DOI:10.1055/s-0033-1338493

Reference yield:

: 1414941-33-5
methyl 2-(2-(4-methoxybenzyloxy)ethyl)oxazole-4-carboxylate

: 1392284-91-1
C₃₄H₅₇NO₇Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogenphosphate / tert-butyl alcohol; water / 1.5 h / 20 °C / Inert atmosphere

2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -30 - 20 °C / Inert atmosphere

3.1: diethylamino-sulfur trifluoride / dichloromethane / -78 - 20 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; Bromotrichloromethane / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

6.1: diethyl ether / 2 h / -100 °C / Inert atmosphere

6.2: 20 °C

7.1: silver(l) oxide / diethyl ether / 18 h / 20 °C / Molecular sieve; Darkness

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0.42 h / 20 °C / Inert atmosphere

9.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

10.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 °C

10.2: 0.67 h / -40 °C

11.1: triethylamine; dicyclohexylboron chloride / diethyl ether; tetrahydrofuran / 1.5 h / -30 °C

11.2: 1.5 h / -78 °C

11.3: 2 h / 0 - 20 °C

12.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

12.2: 0.67 h / 0 °C

With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Bromotrichloromethane; diethylamino-sulfur trifluoride; dicyclohexylboron chloride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; silver(l) oxide; lithium hexamethyldisilazane; isobutyl chloroformate; In tetrahydrofuran; diethyl ether; dichloromethane; water; mineral oil; tert-butyl alcohol;
DOI:10.1055/s-0033-1338493