3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate

Base Information

Chemical Name:3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate
CAS No.:1242275-17-7
Molecular Formula:C₁₆H₂₃NO₃S
Molecular Weight:309.43
Hs Code.:

Synonyms:3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate

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Chemical Property of 3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate

Chemical Property:

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Technology Process of 3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate

There total 4 articles about 3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3-[4-(tert-butoxycarbonylamino)phenyl]propyl methanesulfonate

: 507-09-5
tiolacetic acid

: 1242275-17-7
3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate

Guidance literature:: tiolacetic acid; With potassium tert-butylate; In N,N-dimethyl-formamide;

3-[4-(tert-butoxycarbonylamino)phenyl]propyl methanesulfonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1071/CH09308

Reference yield:

: 198896-23-0
3-(4-tert-butoxycarbonylaminophenyl)propanol

: 1242275-17-7
3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 24 h

2.1: potassium tert-butylate / N,N-dimethyl-formamide

2.2: 48 h / 20 °C

With potassium tert-butylate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1071/CH09308

Reference yield:

: 35271-56-8,142917-82-6,1504-63-8
3-(4-nitrophenyl)propyl-2-en-1-ol

: 1242275-17-7
3-[4-(tert-butoxycarbonylamino)phenyl]propyl ethanethioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium on carbon; hydrogen

2.1: tetrahydrofuran / 24 h / 80 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 24 h

4.1: potassium tert-butylate / N,N-dimethyl-formamide

4.2: 48 h / 20 °C

With palladium on carbon; potassium tert-butylate; hydrogen; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1071/CH09308