C₁₆H₁₃BrO₅

Base Information

Chemical Name:C₁₆H₁₃BrO₅
CAS No.:1335557-44-2
Molecular Formula:C₁₆H₁₃BrO₅
Molecular Weight:365.18
Hs Code.:

C<sub>16</sub>H<sub>13</sub>BrO<sub>5</sub>

Synonyms:C₁₆H₁₃BrO₅

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Chemical Property of C₁₆H₁₃BrO₅

Chemical Property:

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Technology Process of C₁₆H₁₃BrO₅

There total 10 articles about C₁₆H₁₃BrO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254347-09-5
phenyl 6-{[(tert-butoxy)carbonyl]oxy}-4-formyl-3-methoxy-2-methylbenzoate

: 1335557-44-2
C₁₆H₁₃BrO₅

Guidance literature:: phenyl 6-{[(tert-butoxy)carbonyl]oxy}-4-formyl-3-methoxy-2-methylbenzoate; With trifluoroacetic acid; In dichloromethane; at 0 - 10 ℃;

With bromine; sodium acetate; acetic acid; at 10 - 20 ℃;

Reference yield:

: 348169-39-1
4-bromo-2-methoxy-6-methyl-phenylamine

: 1335557-44-2
C₁₆H₁₃BrO₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

1.3: 4 h / 0 - 50 °C

2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

2.2: 0 - 20 °C

3.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

3.2: pH 1

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

5.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

6.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

6.2: 0.33 h / 20 °C

7.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 0 - 20 °C

7.2: 0.33 h / 20 °C

8.1: dmap / dichloromethane / 0.33 h / 20 °C

9.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / 0 °C

9.2: 0.5 h / 0 - 20 °C

10.1: trifluoroacetic acid / dichloromethane / 0 - 10 °C

10.2: 10 - 20 °C

With hydrogenchloride; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; water; isopropylmagnesium chloride; boron tribromide; diisobutylaluminium hydride; triethylamine; trifluoroacetic acid; lithium chloride; sodium nitrite; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1335557-44-2
C₁₆H₁₃BrO₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 0 - 20 °C

6.2: 0.33 h / 20 °C

7.1: dmap / dichloromethane / 0.33 h / 20 °C

8.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / 0 °C

8.2: 0.5 h / 0 - 20 °C

9.1: trifluoroacetic acid / dichloromethane / 0 - 10 °C

9.2: 10 - 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; water; isopropylmagnesium chloride; boron tribromide; diisobutylaluminium hydride; triethylamine; trifluoroacetic acid; lithium chloride; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene; tert-butyl alcohol;