5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine

Base Information

Chemical Name:5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine
CAS No.:1161570-22-4
Molecular Formula:C₂₅H₂₉N₃O₁₃
Molecular Weight:579.518
Hs Code.:

Synonyms:5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine

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Chemical Property of 5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine

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Technology Process of 5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine

There total 3 articles about 5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1145997-23-4
2'-O-acetal levulinyl ester uridine

: 179691-31-7
2-(2-nitrophenyl)propyl chloroformate

: 1161570-22-4
5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine

Guidance literature:: In tetrahydrofuran; pyridine; at 0 ℃; for 3h; Inert atmosphere;

Reference yield:

: 174497-93-9
2'-O-methylthiomethyl-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 1161570-22-4
5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuryl dichloride / benzene; dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / Inert atmosphere

2.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 2 h / Inert atmosphere

3.1: pyridine / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

With pyridine; sulfuryl dichloride; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; dichloromethane; benzene;

Reference yield:

: 1145997-22-3
3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-O-acetal levulinyl ester uridine

: 1161570-22-4
5'-O-2-(2-nitrophenyl)propoxycarbonyl-2'-O-acetal levulinyl ester uridine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 2 h / Inert atmosphere

2: pyridine / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

With pyridine; triethylamine tris(hydrogen fluoride); In tetrahydrofuran;