(S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester

Base Information

Chemical Name:(S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester
CAS No.:83056-89-7
Molecular Formula:C₁₈H₂₄N₂O₅
Molecular Weight:348.399
Hs Code.:

Synonyms:(S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester

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Technology Process of (S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester

There total 3 articles about (S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.4%

: 75-03-6
ethyl iodide

: 77999-24-7
(S)‐2‐oxoimidazolidine‐1,5‐dicarboxylate-5‐tert‐butyl ester-1‐benzyl ester

: 83056-89-7
(S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester

Guidance literature:: In N-methyl-acetamide;

Reference yield:

: 64-67-5
diethyl sulfate

: 77999-24-7
(S)‐2‐oxoimidazolidine‐1,5‐dicarboxylate-5‐tert‐butyl ester-1‐benzyl ester

: 83056-89-7
(S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester

Guidance literature:: With potassium carbonate; In acetone; for 5h; Reflux;

Reference yield:

: 59760-01-9,76497-31-9,46961-70-0
(S)-2-oxo-imidazolidine-1,5-dicarboxylic acid 1-benzyl ester

: 83056-89-7
(S)-3-ethyl-2-oxoimidazolidine-1,5‐dicarboxylic acid 5‐tert‐butyl ester 1‐benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; trichlorophosphate; hydrogenchloride / chloroform / 1 h / 0 °C / pH 3 - 4

2: potassium carbonate / acetone / 5 h / Reflux

With pyridine; hydrogenchloride; potassium carbonate; trichlorophosphate; In chloroform; acetone;