di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

Base Information

Chemical Name:di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane
CAS No.:1396506-65-2
Molecular Formula:C₂₂H₄₁FO₂Si₂
Molecular Weight:412.736
Hs Code.:

Synonyms:di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

Suppliers and Price of di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

There total 3 articles about di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 558-63-4
di-tert-butyldifluorosilane

: 201150-66-5
[(5-bromo-2-methoxyphenyl)methoxy]dimethyl(1,1-dimethylethyl)silane

: 1396506-65-2
di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

Guidance literature:: [(5-bromo-2-methoxyphenyl)methoxy]dimethyl(1,1-dimethylethyl)silane; With tert.-butyl lithium; In diethyl ether; at -78 ℃; for 0.166667h;

di-tert-butyldifluorosilane; In diethyl ether; at -78 - 20 ℃; for 19h;
DOI:10.3390/molecules16097458

Reference yield:

: 25016-01-7
5-bromo-2-methoxybenzaldehyde

: 1396506-65-2
di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol; water / 24 h / 20 °C

2.1: 1H-imidazole / dichloromethane / 20 h / 20 °C

3.1: tert.-butyl lithium / diethyl ether / 0.17 h / -78 °C

3.2: 19 h / -78 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; tert.-butyl lithium; In methanol; diethyl ether; dichloromethane; water;
DOI:10.3390/molecules16097458

Reference yield:

: 80866-82-6
5-bromo-2-methoxy-benzyl alcohol

: 1396506-65-2
di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / dichloromethane / 20 h / 20 °C

2.1: tert.-butyl lithium / diethyl ether / 0.17 h / -78 °C

2.2: 19 h / -78 - 20 °C

With 1H-imidazole; tert.-butyl lithium; In diethyl ether; dichloromethane;
DOI:10.3390/molecules16097458