(5-Bromo-2-methoxybenzyloxy)-tert-butyldimethylsilane

Base Information

Chemical Name:(5-Bromo-2-methoxybenzyloxy)-tert-butyldimethylsilane
CAS No.:201150-66-5
Molecular Formula:C14H23BrO2Si
Molecular Weight:331.325
Hs Code.:
DSSTox Substance ID:DTXSID101146151

Synonyms:201150-66-5;(5-Bromo-2-methoxybenzyloxy)-tert-butyldimethylsilane;((5-Bromo-2-methoxybenzyl)oxy)(tert-butyl)dimethylsilane;SCHEMBL1145736;DTXSID101146151;5-Bromo-2-methoxybenzyl alcohol, TBDMS derivative;A1-49318;[(5-bromo-2-methoxybenzyl)oxy](t-butyl)dimethylsilane;(5-Bromo-2-methoxy-benzyloxy)-tert-butyl-dimethyl-silane;(5-bromo-2-methoxyphenyl)methoxy-tert-butyl-dimethylsilane;5-Bromo-2-methoxybenzyl alcohol, tert-butyldimethylsilyl ether;4-Bromo-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-1-methoxybenzene

Suppliers and Price of (5-Bromo-2-methoxybenzyloxy)-tert-butyldimethylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (5-Bromo-2-methoxybenzyloxy)-tert-butyldimethylsilane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:330.06507
Heavy Atom Count:18
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OCC1=C(C=CC(=C1)Br)OC

Technology Process of (5-Bromo-2-methoxybenzyloxy)-tert-butyldimethylsilane

There total 5 articles about (5-Bromo-2-methoxybenzyloxy)-tert-butyldimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 80866-82-6
5-bromo-2-methoxy-benzyl alcohol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 201150-66-5
[(5-bromo-2-methoxyphenyl)methoxy]dimethyl(1,1-dimethylethyl)silane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; Cooling with ice;
DOI:10.1055/s-0031-1290899

Reference yield: 89.0%

: 4-bromo-1-(tert-butyl-dimethyl-silanyloxy)-2-(tert-butyl-dimethyl-silanyloxymethyl)-benzene

: 74-88-4
methyl iodide

: 201150-66-5
[(5-bromo-2-methoxyphenyl)methoxy]dimethyl(1,1-dimethylethyl)silane

Guidance literature:: 4-bromo-1-(tert-butyl-dimethyl-silanyloxy)-2-(tert-butyl-dimethyl-silanyloxymethyl)-benzene; With lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1055/s-2003-38744