2-(3, 5-dimethylphenyl)-2H-indazole

Base Information

Chemical Name:2-(3, 5-dimethylphenyl)-2H-indazole
CAS No.:474352-67-5
Molecular Formula:C₁₅H₁₄N₂
Molecular Weight:222.29
Hs Code.:

Synonyms:2-(3, 5-dimethylphenyl)-2H-indazole

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Chemical Property of 2-(3, 5-dimethylphenyl)-2H-indazole

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Technology Process of 2-(3, 5-dimethylphenyl)-2H-indazole

There total 8 articles about 2-(3, 5-dimethylphenyl)-2H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 271-44-3
benzimidazole

: C₁₈H₂₀F₃IO₃S

: 474352-67-5
2-(3, 5-dimethylphenyl)-2H-indazole

Guidance literature:: With copper(l) chloride; In dichloromethane; at 50 ℃; for 12h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c8ob00128f

Reference yield: 87.8%

: 474352-67-5
2-(3, 5-dimethylphenyl)-2H-indazole

Guidance literature:: With copper(l) chloride; In dichloromethane; at 50 ℃; for 12h; Schlenk technique; Inert atmosphere;

Reference yield: 77.0%

: 39943-61-8
3,5-dimethylphenylhydrazine

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 474352-67-5
2-(3, 5-dimethylphenyl)-2H-indazole

Guidance literature:: 3,5-dimethylphenylhydrazine; 1-Bromo-2-bromomethyl-benzene; With caesium carbonate; In dimethyl sulfoxide; at 20 ℃; for 3h; Inert atmosphere; Sealed tube;

With caesium carbonate; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate; In dimethyl sulfoxide; at 120 ℃; for 18h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.0c01923