C₂₄H₂₂Cl₂O₄

Base Information

Chemical Name:C₂₄H₂₂Cl₂O₄
CAS No.:1335557-47-5
Molecular Formula:C₂₄H₂₂Cl₂O₄
Molecular Weight:445.342
Hs Code.:

C<sub>24</sub>H<sub>22</sub>Cl<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₄H₂₂Cl₂O₄

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Chemical Property of C₂₄H₂₂Cl₂O₄

Chemical Property:

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Technology Process of C₂₄H₂₂Cl₂O₄

There total 13 articles about C₂₄H₂₂Cl₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335557-46-4
C₂₄H₂₄O₆

: 1335557-47-5
C₂₄H₂₂Cl₂O₄

Guidance literature:: With thionyl chloride; tetrabutyl-ammonium chloride; In 1,2-dichloro-ethane; at 80 ℃; for 1.5h; Sealed;

Reference yield:

: 348169-39-1
4-bromo-2-methoxy-6-methyl-phenylamine

: 1335557-47-5
C₂₄H₂₂Cl₂O₄

Guidance literature:: Multi-step reaction with 13 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

1.3: 4 h / 0 - 50 °C

2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

2.2: 0 - 20 °C

3.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

3.2: pH 1

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

5.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

6.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

6.2: 0.33 h / 20 °C

7.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 0 - 20 °C

7.2: 0.33 h / 20 °C

8.1: dmap / dichloromethane / 0.33 h / 20 °C

9.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / 0 °C

9.2: 0.5 h / 0 - 20 °C

10.1: trifluoroacetic acid / dichloromethane / 0 - 10 °C

10.2: 10 - 20 °C

11.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 0 °C

11.2: 0.5 h / 0 °C

12.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

12.2: 0.5 h / 0 °C

13.1: thionyl chloride; tetrabutyl-ammonium chloride / 1,2-dichloro-ethane / 1.5 h / 80 °C / Sealed

With hydrogenchloride; dmap; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; tetrabutyl-ammonium chloride; water; isopropylmagnesium chloride; boron tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; lithium chloride; sodium nitrite; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1335557-47-5
C₂₄H₂₂Cl₂O₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 0 - 20 °C

6.2: 0.33 h / 20 °C

7.1: dmap / dichloromethane / 0.33 h / 20 °C

8.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / 0 °C

8.2: 0.5 h / 0 - 20 °C

9.1: trifluoroacetic acid / dichloromethane / 0 - 10 °C

9.2: 10 - 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 0 °C

10.2: 0.5 h / 0 °C

11.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

11.2: 0.5 h / 0 °C

12.1: thionyl chloride; tetrabutyl-ammonium chloride / 1,2-dichloro-ethane / 1.5 h / 80 °C / Sealed

With dmap; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; tetrabutyl-ammonium chloride; water; isopropylmagnesium chloride; boron tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; lithium chloride; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;