Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}

Base Information

Chemical Name:Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}
CAS No.:188058-80-2
Molecular Formula:C₃₁H₂₈N₄O₆S₂
Molecular Weight:616.719
Hs Code.:

Synonyms:Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}

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Chemical Property of Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}

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Technology Process of Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}

There total 3 articles about Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 142-79-0
pimeloyl chloride

: 93352-49-9
4-amino-2'-nitrodiphenyl sulfide

: 188058-80-2
Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}

Guidance literature:: With pyridine; 1) 0 deg C, 1 h; 2) rt, 7 h;
DOI:10.1016/S0223-5234(97)84360-7

Reference yield:

: 22948-02-3
3-aminothiophenol

: 188058-80-2
Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / sodium acetate / ethanol / 36 h / Heating

2: 93 percent / pyridine / 1) 0 deg C, 1 h; 2) rt, 7 h

With pyridine; sodium acetate; In ethanol;
DOI:10.1016/S0223-5234(97)84360-7

Reference yield:

: 88-73-3
2-Chloronitrobenzene

: 188058-80-2
Heptanedioic acid bis-{[3-(2-nitro-phenylsulfanyl)-phenyl]-amide}

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / sodium acetate / ethanol / 36 h / Heating

2: 93 percent / pyridine / 1) 0 deg C, 1 h; 2) rt, 7 h

With pyridine; sodium acetate; In ethanol;
DOI:10.1016/S0223-5234(97)84360-7