N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine

Base Information

• Chemical Name: N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine
• CAS No.: 73074-23-4
• Molecular Formula: C₂₀H₁₉N₃O₇S
• Molecular Weight: 445.453

Synonyms:N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine

Chemical Property of N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine

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Technology Process of N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine

There total 1 articles about N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine (47364-78-3) → N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine (73074-23-4)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; Ambient temperature;

DOI:10.1016/S0008-6215(00)83661-7

Reference yield: 78.0%

9-(5-amino-2,3,5-trideoxy-β-D-glycero-pent-2-enofuranosyl)adenine (62748-93-0) + N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine (73074-23-4) → (S)-N-[(2S,5R)-5-(6-Amino-purin-9-yl)-2,5-dihydro-furan-2-ylmethyl]-3-(4-methoxy-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionamide (73074-28-9)

Guidance literature:

In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1016/S0008-6215(00)83661-7

Reference yield: 75.0%

N-hydroxysuccinimide ester of O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine (73074-23-4) + 1-(5-amino-2,3,5-trideoxy-β-D-glycero-pent-2-enofuranosyl)cytosine (62748-91-8) → (S)-N-[(2S,5R)-5-(4-Amino-2-oxo-2H-pyrimidin-1-yl)-2,5-dihydro-furan-2-ylmethyl]-3-(4-methoxy-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionamide (73074-25-6)

Guidance literature:

In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1016/S0008-6215(00)83661-7

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

O-methyl-N-(o-nitrophenylsulfenyl)-L-tyrosine

Downstream raw materials:

(S)-N-[(2S,5R)-5-(6-Amino-purin-9-yl)-2,5-dihydro-furan-2-ylmethyl]-3-(4-methoxy-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionamide

(S)-N-[(2S,5R)-5-(4-Amino-2-oxo-2H-pyrimidin-1-yl)-2,5-dihydro-furan-2-ylmethyl]-3-(4-methoxy-phenyl)-2-(2-nitro-phenylsulfanylamino)-propionamide

(S)-2-Amino-N-[(2S,5R)-5-(6-amino-purin-9-yl)-2,5-dihydro-furan-2-ylmethyl]-3-(4-methoxy-phenyl)-propionamide

(S)-2-Amino-N-[(2S,5R)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-2,5-dihydro-furan-2-ylmethyl]-3-(4-methoxy-phenyl)-propionamide

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