7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c][1,4]oxazine-1,6-dione

Base Information

Chemical Name:7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c][1,4]oxazine-1,6-dione
CAS No.:1402004-16-3
Molecular Formula:C₁₂H₁₁N₃O₃
Molecular Weight:245.238
Hs Code.:

Synonyms:7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c]-[1,4]oxazine-1,6-dione

Suppliers and Price of 7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c][1,4]oxazine-1,6-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 10 raw suppliers

Chemical Property of 7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c][1,4]oxazine-1,6-dione

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c][1,4]oxazine-1,6-dione

There total 13 articles about 7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c][1,4]oxazine-1,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1402003-83-1
5-(4-Methyl-1H-imidazol-1-yl)-6-oxo-1,6-dihydropyridine-2-carboxylic acid, hydrochloride salt

: 106-93-4
ethylene dibromide

: 1402004-16-3
7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c]-[1,4]oxazine-1,6-dione

Guidance literature:: With caesium carbonate; In dichloromethane; at 90 ℃; for 6h;

Reference yield: 71.0%

: 822-36-6
4-methyl-1H-imidazole

: 7-bromo-3,4-dihydropyrido[2, 1-c][1,4]oxazine-1,6-dione

: 1402004-16-3
7-(4-methyl-1H-imidazol-1-yl)-3,4-dihydropyrido[2,1-c]-[1,4]oxazine-1,6-dione

Guidance literature:: With methanesulfonato[9,9-dimethyl-4,5-bis-(diphenylphosphino)xanthene](2'-methylamino-1,1'-biphenyl-2-yl)-palladium(II); potassium hydrogencarbonate; In 1,4-dioxane; toluene; for 16h; Reagent/catalyst; Molecular sieve; Inert atmosphere; Reflux;
DOI:10.1021/acs.joc.8b02953