O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

Base Information

Chemical Name:O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol
CAS No.:224784-99-0
Molecular Formula:C₄₅H₄₀O₇
Molecular Weight:692.808
Hs Code.:

O<sup>3</sup>-(3-carboxypropionyl)-O<sup>1</sup>-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

Synonyms:O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

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Chemical Property of O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

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Technology Process of O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

There total 7 articles about O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 108-30-5
succinic acid anhydride

: 224784-97-8
O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

: 224784-99-0
O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

Guidance literature:: With pyridine; dmap;

Reference yield:

: 197722-93-3
pentafluorophenyl 2-(pyren-1-yl)acetate

: 224784-99-0
O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / Et₃N / tetrahydrofuran / 1 h / 20 °C

2: 86 percent / TFA / 0.5 h / Heating

3: 87 percent / NaBH₄ / tetrahydrofuran; methanol / Heating

4: 80 percent / pyridine / 1 h / 20 °C

5: 94 percent / DMAP / 120 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1: Condensation / 2: Ring cleavage / 3: Reduction / 4: Substitution / 5: Acylation;
DOI:10.1080/07328319908044632

Reference yield:

: 199920-11-1
ethyl 4-(1-pyrenyl)-3-oxobutanoate

: 224784-99-0
O³-(3-carboxypropionyl)-O¹-(4,4'-dimethoxytrityl)-4-(1-pyrenyl)-1,3-butanediol

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / NaBH₄ / tetrahydrofuran; methanol / Heating

2: 80 percent / pyridine / 1 h / 20 °C

3: 94 percent / DMAP / 120 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; In tetrahydrofuran; methanol; 1: Reduction / 2: Substitution / 3: Acylation;
DOI:10.1080/07328319908044632