S-benzoyl-mercaptoacetic acid N,N-dimethylamide

Base Information

Chemical Name:S-benzoyl-mercaptoacetic acid N,N-dimethylamide
CAS No.:318257-78-2
Molecular Formula:C₁₁H₁₃NO₂S
Molecular Weight:223.296
Hs Code.:

Synonyms:S-benzoyl-mercaptoacetic acid N,N-dimethylamide

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Chemical Property of S-benzoyl-mercaptoacetic acid N,N-dimethylamide

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Technology Process of S-benzoyl-mercaptoacetic acid N,N-dimethylamide

There total 1 articles about S-benzoyl-mercaptoacetic acid N,N-dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 98-91-9
thiobenzoic acid

: 2675-89-0
2-chloro-N,N-dimethylacetamide

: 318257-78-2
S-benzoyl-mercaptoacetic acid N,N-dimethylamide

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1021/ja005613q

Reference yield: 88.0%

: 5720-06-9
2-Methoxyphenylboronic acid

: 318257-78-2
S-benzoyl-mercaptoacetic acid N,N-dimethylamide

: 2553-04-0
ortho-methoxybenzophenone

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane; In tetrahydrofuran; at 50 ℃; for 18h;
DOI:10.1021/ja005613q

Reference yield: 88.0%

: 1292766-17-6
copper(I) thiophene-2-carboxylate

: 5720-06-9
2-Methoxyphenylboronic acid

: 318257-78-2
S-benzoyl-mercaptoacetic acid N,N-dimethylamide

: B(OH)2(C₄H₃SCOO)

: Cu⁽¹⁺⁾*SCH₂CON(CH₃)2^(1-)=CuSCH₂CON(CH₃)2

: 2553-04-0
ortho-methoxybenzophenone

Guidance literature:: With Pd₂(dba)3*CHCl₃/tris(2-furyl)phosphine; In tetrahydrofuran; addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of PhCOSCH2CONMe2 (1 equiv.) with CH3OC6H4B(OH)2 (1 equiv.) in THF in presence of 1% Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
DOI:10.1021/ja005613q