4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Base Information

Chemical Name:4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide
CAS No.:1450923-21-3
Molecular Formula:C₁₆H₁₆N₄O₄S₂
Molecular Weight:392.459
Hs Code.:

Synonyms:4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

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Chemical Property of 4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

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Technology Process of 4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

There total 6 articles about 4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450923-20-2
3-fluoro-N-(4-methoxybenzyl)-4-nitro-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

: 1450923-21-3
4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium trimethylsilanolate / tetrahydrofuran / 0 °C

2: acetic acid; iron / tetrahydrofuran / 40 h / Sealed tube; Heating

With sodium trimethylsilanolate; iron; acetic acid; In tetrahydrofuran;

Reference yield:

: C₁₆H₁₄N₄O₆S₂

: 1450923-21-3
4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Guidance literature:: With iron; acetic acid; In tetrahydrofuran; for 40h; Sealed tube; Heating;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1450923-21-3
4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triisopropoxytitanium(IV) chloride / dichloromethane / 3 h

1.2: 1 h / 0 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

2.2: 0.25 h / -78 °C

3.1: sodium trimethylsilanolate / tetrahydrofuran / 0 °C

4.1: acetic acid; iron / tetrahydrofuran / 40 h / Sealed tube; Heating

With triisopropoxytitanium(IV) chloride; sodium trimethylsilanolate; iron; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;